|
NMR
Solvent Shifts (in ppm) and Solvent Spectra
|
Solvent
|
Proton
|
J
(H-D), Hz
|
Carbon
|
J
(C-D), Hz
|
m. p. (oC)
|
b. p.
(oC)
|
Viscosity |
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
| |
|
|
|
|
|
|
|
|
Acetic Acid-d4
|
11.53
(1)
2.03
(5)
|
2
|
178.4
(br)
20.0
(7)
|
20
|
17
|
118
|
|
|
Acetone-d6
|
2.04
(5)
|
2.2
|
206.0
(13)
29.8
(7)
|
0.9
20
|
-94
|
57
|
|
|
Acetonitrile-d3
|
1.93
(5)
|
2.5
|
118.2
(Br)
1.3
(7)
|
21
|
-45
|
82
|
|
|
Benzene-d6
|
7.15
(Br)
|
-
|
128.0
(3)
|
24
|
5
|
80
|
|
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